HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloral Hydrate → HCID 57046400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloral Hydrate | HCID 2707 | — |
| Reactant | P-Toluenesulfonylhydrazide | HCID 15303 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57046400 | HCID 57046400 | — |
Reaction Steps
In 20 ml of methanol were dissolved 3.98 g (24 mmole) of chloral hydrate and 3.72 g (20 mmole) of p-toluenesulfonylhydrazine, and the mixture was stirred at room temperature for 40 minutes to form trichloroacetaldehyde-p-toluenesulfonylhydrazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675412 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-7bd7460f5edd46cfb4b71e9e4f278180 |
| Source note | uspto-grants-1987_06 |