HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20027805, compound → HCID 20027819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20027805 | HCID 20027805 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20027819 | HCID 20027819 | — |
Reaction Steps
In a manner analogous to that described in Example 1a, 2.3 g of 3-isopropyl-1-(4-nitrophenyl)-3-azabicyclo[-3.1.1]-heptane-2,4-dione are dissolved in 50 ml of ethyl acetate, hydrogenated in the presence of 0.25 g of 5% palladium-on-carbon and worked up. Melting point 191°-201° (from ethyl acetate/hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04677129 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-b20c245036a445d3a06662ab4a9ebc16 |
| Source note | uspto-grants-1987_06 |