HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20027830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 20027828 | HCID 20027828 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | HCID 20027830 | HCID 20027830 | — |
Reaction Steps
In a manner analogous to that described in Example 12a, 3.7 g of 5-methyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione in 80 ml of 2-methoxyethanol are hydrogenated in the presence of 0.4 g of 5% palladium-on-carbon and worked up. Melting point 216° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04677129 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-f50d021703884aa587913d6857e3085a |
| Source note | uspto-grants-1987_06 |