HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloro-3-nitrotoluene → 3-Chloro-2-methyl-6-nitrobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloro-3-nitrotoluene | HCID 97155 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 3-Bromo-2-methyl-6-nitrobenzonitrile | HCID 13885407 | — |
| Product | 3-Chloro-2-methyl-6-nitrobenzonitrile | HCID 22008961 | — |
Reaction Steps
The title compound was prepared using the method described above for preparing 3-bromo-2-methyl-6-nitrobenzonitrile, except that the reaction was carried out at 210° C. and employed 2,6-dichloro-3-nitrotoluene as the starting material. The infrared spectrum of a potassium bromide pellet of the product exhibited principal absorption peaks at 3121, 2231, 1602, 1560, 1530, and 1348 receiprocal centimeters.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04677219 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-f605f8faf8b5490ebba211bea74f31dd |
| Source note | uspto-grants-1987_06 |