HRID653538

反应详情

EQUATION

反应方程式

HRID 653538 的结构方程式

PROCEDURE

实验过程

The title compound was prepared using the method described above for preparing 3-bromo-2-methyl-6-nitrobenzonitrile, except that the reaction was carried out at 210° C. and employed 2,6-dichloro-3-nitrotoluene as the starting material. The infrared spectrum of a potassium bromide pellet of the product exhibited principal absorption peaks at 3121, 2231, 1602, 1560, 1530, and 1348 receiprocal centimeters.

WORKUP

后处理

  1. customwas carried out at 210° C.
  2. customabsorption peaks at 3121, 2231, 1602, 1560, 1530, and 1348 receiprocal centimeters