HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13070187, compound → HCID 19889136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13070187 | HCID 13070187 | — |
| Reactant | HCID 178418373 | HCID 178418373 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19889136 | HCID 19889136 | 89% |
Reaction Steps
9-anthrylacetaldehyde (1.1 g; 5 mmoles) was Soxhlet--extracted for a period of 6 hours in an ether solution (100 ml) of methylmagnesium iodide (30 mmoles; prepared from 0.72 g of magnesium). Work up as described above gave 1.05 g (89%) of 1-(9-anthryl)-2-propanol as pale yellow needle shaped crystals, mp 105°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128120 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-526e854b716442f18046fbb4ff1dc6f8 |
| Source note | uspto-grants-1992_07 |