HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 653608Generated: October 29, 2026
Dimethylformamide → HCID 136037622, compound
https://huagongshe.com/reaction/653608
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 4-aminoquinazolin-2-ol | HCID 11958943 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 136037622 | HCID 136037622 | — |
Reaction Steps
1.61 g (0.01 mol) of 4-amino-2-quinazolinone and then 2.2 g (0.011 mol) of phenacyl bromide are added to 25 ml of dimethylformamide. The mixture is heated at 120° C. (external heating) for 3 hours, then left to cool and water is added. The brown precipitate formed is filtered out (1.34 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05128338 |
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| Source dataset | uspto-grants-1992_07 |
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| ORD ID | ord-07ea7bf8f97b4f1a9673ea5d74580416 |
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| Source note | uspto-grants-1992_07 |
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