HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 7H-Naphtho(1,2,3-ij)(2,7)naphthyridin-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 4-Methylbenzo(g)quinoline-5,10-dione | HCID 457732 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 7H-Naphtho(1,2,3-ij)(2,7)naphthyridin-7-one | HCID 387195 | — |
Reaction Steps
Dimethylformamide dimethyl acetal (1.50 mL, 11.34 mmol, Aldrich) was added to a solution of cleistopholine, (1.95 g, 8.73 mmol) in dimethylformamide (5 mL). The mixture was then heated for 30 min by submerging
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128344 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-77d63ea9d6e74c1ebb14483c828a2966 |
| Source note | uspto-grants-1992_07 |