Hydrochloric Acid → HCID 19889695, compound

Participants

Reaction Steps

4.84 g (30 mmol) of 2,3-dimethylphenoxy-acetonitrile, 3.3 g (33 mmol) of N-allyl-ethylenediamine and 260 mg of sodium polysulfide (Na2S4) are stirred together at 50° C. for 4 hours. The excess amine is then stripped off under a high vacuum, ethanolic hydrochloric acid is added to the residue and the hydrochloride is precipitated by addition of ether.

Provenance & Evidence