Acetonitrile → HCID 88147654, compound

Participants

Reaction Steps

The compound (0.5 g) of Example 23 was dissolved at room temperature in a 4% (w/v) hydrochloric acid-methanol solution (5 ml), followed by stirring for 1 hour. Acetonitrile (50 ml) was added, and a precipitate thus formed was collected by filtration. The precipitate was washed with acetonitrile and acetone to obtain the target product (0.31 g). Infrared spectrum (cm-1, Nujol): 1780, 1690.

Provenance & Evidence