Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Oleic Acid | HCID 445639 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131716512 | HCID 131716512 | — |
Reaction Steps
770 g of glycerine and 767 g of oleic acid were treated with catalyst prepared in a similar way as in Example 4. 4 g of Ca(OH)2 (dry) premixed with 26 g of water and 15 g of 25% H3PO4 premixed with 30 g of water were added at room temperature. The batch was heated to 230° C. under 23 inches of maximum vacuum in 2 hours time and reacted for another 3 hours. 240 g of total water was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05130060 |
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| Source dataset | uspto-grants-1992_07 |
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| ORD ID | ord-189caeecaf694f89af3c9f942413fb2d |
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| Source note | uspto-grants-1992_07 |
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