HRID654053
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Analogously to Example 21(b), 2.41 g (8 mmol) of 3-fluoro-6-(trifluoromethylsulfamoyl)-benzoic acid methyl ester in aqueous dioxane is saponified with NaOH and isolated. 1.55 g=67.3% of the theoretical yield is obtained as a partially crystalline product.
WORKUP
后处理
- customisolated
- custom1.55 g=67.3% of the theoretical yield
- customis obtained as a partially crystalline product