HRID654053

反应详情

EQUATION

反应方程式

HRID 654053 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Analogously to Example 21(b), 2.41 g (8 mmol) of 3-fluoro-6-(trifluoromethylsulfamoyl)-benzoic acid methyl ester in aqueous dioxane is saponified with NaOH and isolated. 1.55 g=67.3% of the theoretical yield is obtained as a partially crystalline product.

WORKUP

后处理

  1. customisolated
  2. custom1.55 g=67.3% of the theoretical yield
  3. customis obtained as a partially crystalline product