HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodiphenylmethane → 1,3-Dichloro-2-diphenylmethoxypropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodiphenylmethane | HCID 7035 | — |
| Reactant | 1,3-Dichloro-2-propanol | HCID 7289 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1,3-Dichloro-2-diphenylmethoxypropane | HCID 12329338 | 80% |
Reaction Steps
A stirred solution of 508 g (2.5 mol) of diphenylmethylchloride and 387 g (3 mol) of 1,3-dichloro-2-propanol in 700 mL of dry toluene was heated at reflux temperature for 72 hr. The reaction mixture was concentrated in vacuo and the residual oil distilled to give 587 g (80%) of colorless oil; bp 137°-140° C./0.1 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05130309 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-a5ec3514365444e2a402bb23cb6688dd |
| Source note | uspto-grants-1992_07 |