HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 15056485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 15056489 | HCID 15056489 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 15056485 | HCID 15056485 | — |
Reaction Steps
A mixture of 2.98 g of 2-methoxymethyl-2-methyl-4-(1,2-dihydro-2-oxo-1-pyridyl)-6-carbamoylchroman, 2 ml of POCl3 and 200 ml of 1,2-dichloroethane is boiled for 45 min. Cooling and customary working up gives 2-methoxymethyl-2-methyl-4-(1,2-dihydro-2-oxo-1-pyridyl)-6-cyanochroman.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05130322 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-ca5159ed42134bf3b7305f14ab02e546 |
| Source note | uspto-grants-1992_07 |