HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 15718589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 15718588 | HCID 15718588 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15718589 | HCID 15718589 | — |
Reaction Steps
A mixture of the product obtained in step (i) (23.8 g, 0.11 mol) and hydroxylamine hydrochloride (8.2 g, 0.12 mol) in methanol (300 ml) is refluxed for ten minutes and then evaporated off under vacuum. Water is added thereto and the mixture is extracted with ethyl ether affording 19 g of the compound indicated in the title; m.p. 84°-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05130339 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-fa46b724462049768430a5f824b7c26d |
| Source note | uspto-grants-1992_07 |