Glycerol → HCID 14229398, compound

HRID 654254Notes

Reaction equation

[B:1]([OH:4])([OH:3])[OH:2].[OH:5][CH2:6][CH:7]([CH2:9]O)[OH:8]>>[B:1]([O:4][CH2:9][CH:7]([CH2:6][OH:5])[OH:8])([OH:3])[OH:2]

Participants

Reactant 2

HCID 753Glycerol

HCID 7628Boric Acid

Product 1

HCID 14229398HCID 14229398, compound

Conditions

Temperature: 180 fahrenheit

Procedure

The glycerol borate acid salt of TEDA was prepared according to U.S. Pat. No. 3,113,515. Boric acid was combined with 2 molar equivalents of glycerol and heated to 180° F. to afford a glycerol borate acid. The reaction mixture was then cooled to 100° F. and treated with 1 molar equivalent of TEDA. Further cooling afforded a viscous material containing 30 wt% TEDA which had a measured Brookfield viscosity of 14,800 centipoise at 25° C.

Workup

customThe glycerol borate acid salt of TEDA was prepared

Sources & evidence

ORD record: ord-38eb9cb7fed0472292104396c88df3d3
Source dataset: uspto-grants-1992_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05130403

Reaction notes

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