Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Boric Acid | HCID 7628 | — |
| Product | HCID 14229398 | HCID 14229398 | — |
Reaction Conditions
| Temperature | 180 fahrenheit |
|---|
Reaction Steps
The glycerol borate acid salt of TEDA was prepared according to U.S. Pat. No. 3,113,515. Boric acid was combined with 2 molar equivalents of glycerol and heated to 180° F. to afford a glycerol borate acid. The reaction mixture was then cooled to 100° F. and treated with 1 molar equivalent of TEDA. Further cooling afforded a viscous material containing 30 wt% TEDA which had a measured Brookfield viscosity of 14,800 centipoise at 25° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05130403 |
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| Source dataset | uspto-grants-1992_07 |
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| ORD ID | ord-38eb9cb7fed0472292104396c88df3d3 |
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| Source note | uspto-grants-1992_07 |
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