Tetrahydrofuran → HCID 86745983, compound

HRID 654259Notes

Reaction equation

HRID 654259 reaction equation
[F:1][Sb-:2]([F:7])([F:6])([F:5])([F:4])[F:3].[Fe+2:8].C(O)(=O)C.[F:13][Sb-:14]([F:19])([F:18])([F:17])([F:16])[F:15].[CH2:20]1[CH2:24][O:23][CH2:22][CH2:21]1>>[F:1][Sb-:2]([F:7])([F:6])([F:5])([F:4])[F:3].[Fe+2:8].[O:23]1[CH2:24][CH2:20][CH2:21][CH2:22]1.[F:13][Sb-:14]([F:19])([F:18])([F:17])([F:16])[F:15]

Participants

3

Reactant 2

HCID 8028TetrahydrofuranHCID 86745984HCID 86745984, compound

Product 1

HCID 86745983HCID 86745983, compound

Procedure

1.0 g of (acetic acid)-iron(II) hexafluoroantimonate are suspended in 10 ml of THF and the suspension is refluxed for 5 minutes. After cooling to room temperature, the product is filtered off under an inert gas and washed with THF. 0.95 g of white, very hygroscopic product results.

Workup

  1. temperaturethe suspension is refluxed for 5 minutes
  2. filtrationthe product is filtered off under an inert gas
  3. washwashed with THF
  4. custom0.95 g of white, very hygroscopic product results

Sources & evidence

ORD record
ord-ef6232746956443caa4abf66b28a824e
Source dataset
uspto-grants-1992_07
Patent number
US05130406

Reaction notes

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