HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 2054580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Mercaptobenzoic Acid | HCID 5443 | — |
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 2054580 | HCID 2054580 | — |
Reaction Steps
To thiosalicylic acid (77 g) slurried in methyl ethyl ketone (500 ml) was added 1 equivalent of K2CO3 followed by 3-bromopropyne (1 equivalent). The reaction mixture was stirred for 3 hours and then poured into 1N HCl and the solids filtered and then vacuum dried to afford the subtitle compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05130485 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-d40b49e8a13b43429115b31ce5cdeb2a |
| Source note | uspto-grants-1992_07 |