HCID 54294522, compound → HCID 19887623, compound

Participants

Reaction Steps

A mixture of 4-[2-(N-methyl-N-phenylamino)ethoxy]benzyl alcohol (3.36 g), manganese (IV) oxide (11.3 g) and dichloromethane (150 ml) were stirred at room temperature overnight. The mixture was filtered through a Soxhlet thimble and the residue extracted with refluxing dichloromethane for 2.5 hours. The solvent was evaporated to afford the title compound, an oil, which was used without further purification.

Provenance & Evidence