HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium 2-chloro-3-benzyloxypropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-(Benzyloxy)-2-chloropropanoic acid | HCID 19887795 | — |
| Solvent | Water | HCID 962 | — |
| Product | Sodium 2-chloro-3-benzyloxypropionate | HCID 23721614 | — |
Reaction Steps
85 g of 2-chloro-3-benzyloxypropionic acid (0.396 mol) were suspended in 550 ml of water and neutralized to pH 7 with 10% sodium hydroxide. After stirring for 15 min, the resulting aqueous solution was washed with ethyl ether and evaporated to dryness under vacuum to give the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05132409 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-ce6d7bc3a6f446ad8c73792b287efab1 |
| Source note | uspto-grants-1992_07 |