N-vinyl-2-pyrrolidone → HCID 178435876, compound

HRID 654648Notes

Reaction equation

HRID 654648 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[N:2]1.[CH:10]([N:12]1[CH2:16][CH2:15][CH2:14][C:13]1=[O:17])=[CH2:11]>>[O:17]=[C:13]1[CH2:14][CH2:15][CH2:16][N:12]1[CH:10]([C:9]1[C:4]2[N:3]=[N:2][NH:1][C:5]=2[CH:6]=[CH:7][CH:8]=1)[CH3:11]

Participants

3

Reactant 2

HCID 6917N-vinyl-2-pyrrolidoneHCID 178418385HCID 178418385, compound

Product 1

HCID 178435876HCID 178435876, compoundYield 64%

Procedure

This product is synthesised, in 64% yield, from benzotriazole and 1-vinyl-2-pyrrolidinone by the same method described in Example 1. The product distils at 180°/0.05 mbar and solidifies, on standing, to yield a white solid mp 77°-9° C.

Workup

  1. customThe product distils at 180°/0.05 mbar

Sources & evidence

ORD record
ord-de9199a7ff424775b3fbf7b057c3f74f
Source dataset
uspto-grants-1992_07
Patent number
US05133890

Reaction notes

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