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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 654760Generated: October 30, 2026

Dimethylformamide → HCID 19761210, compound

https://huagongshe.com/reaction/654760

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamideHCID 6228—
ReactantHCID 19761227HCID 19761227—
SolventWaterHCID 962—
ProductHCID 19761210HCID 19761210—

Reaction Conditions

Temperature150 °C

Reaction Steps

0.046 mole of the acid obtained in stage B is mixed with 19 ml of dimethylformamide and the mixture is then heated to 150° C. for 2 hours. The mixture is taken up with water and the product is extracted with ethyl ether. The organic phases are washed with sodium bicarbonate solution and then with water; they are dried and the solvent is evaporated off to obtain an oily residue.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05134147
Source datasetuspto-grants-1992_07
ORD IDord-3f35a3d3b8f5488296693e161defe189
Source noteuspto-grants-1992_07