HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Anilinonicotinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Chloronicotinic acid | HCID 76258 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 2-Anilinonicotinic acid | HCID 1481799 | — |
Reaction Steps
50 ml of distilled aniline and 43.2 g of 2-chloronicotinic acid are mixed in 126 ml of xylene. The mixture is brought to reflux for 4 hours. It is allowed to cool and the precipitate is filtered off and washed several times with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134147 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-247b5eb095e94e598a5e02792dc86374 |
| Source note | uspto-grants-1992_07 |