HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 10643405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 10498716 | HCID 10498716 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10643405 | HCID 10643405 | — |
Reaction Steps
A mixture of 1-(4-fluorophenyl)-5-[4-(methylsulfonyl)phenyl]pyrazole-3-carboxylic acid (6.4 g) and thionyl chloride (30 ml) in tetrahydrofuran (60 ml) was refluxed for 1 hour and concentrated under reduced pressure, giving 1-(4-fluorophenyl)-5-[4-(methylsulfonyl)phenyl]pyrazole-3-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134142 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-e14af48efe4f4b22b34db7842707a432 |
| Source note | uspto-grants-1992_07 |