HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11791912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 10782496 | HCID 10782496 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 11791912 | HCID 11791912 | — |
Reaction Steps
A mixture of 1-(4-fluorophenyl)-5-[4-(methylthio)phenyl]pyrazole-3-carboxylic acid (13.5 g) and thionyl chloride (10 ml) in dichloroethane (30 ml) was refluxed for 1 hour. The mixture was concentrated to give an oil of 1-(4-fluorophenyl)-5-[4-(methylthio)phenyl]pyrazole-3-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134142 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-0a78bff5cb7c4ba8abd600a8b26ba007 |
| Source note | uspto-grants-1992_07 |