HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2,4-difluorophenyl)-4-(methanesulfonyloxy)-4-methyl-(1H-1,2,4-triazol-1-yl)-2-butanol → HCID 15008578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2,4-difluorophenyl)-4-(methanesulfonyloxy)-4-methyl-(1H-1,2,4-triazol-1-yl)-2-butanol | HCID 19886509 | — |
| Reactant | HCID 178418473 | HCID 178418473 | — |
| Product | HCID 15008578 | HCID 15008578 | — |
Reaction Steps
Following a procedure similar to that described in Example 4, but using 590 mg of 2-(2,4-difluorophenyl)-4-(methanesulfonyloxy)-4-methyl-(1H-1,2,4-triazol-1-yl)-2-butanol (which was synthesized from allylmagnesium chloride in a similar manner to the procedure described in Japanese Patent Provisional Publication No. Sho 59-517 and Preparations 2, 3 and 4), one of the stereoisomers at the C4 position was obtained as the major product in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134152 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-9405083c0f204477b11eb08fc4557b76 |
| Source note | uspto-grants-1992_07 |