HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethyl-2-butene → 2-(2,4'-Difluorophenyl)-3,3,4,4-tetramethyl-2-[(1H-1,2,4-triazol-1-yl)methyl]oxetane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethyl-2-butene | HCID 11250 | — |
| Reactant | 1-(2,4-Difluorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone | HCID 588080 | — |
| Product | 2-(2,4'-Difluorophenyl)-3,3,4,4-tetramethyl-2-[(1H-1,2,4-triazol-1-yl)methyl]oxetane | HCID 15008615 | 15% |
Reaction Steps
Following a procedure similar to that described in Example 39, but using 2,3-dimethyl-2-butene and 2',4'-difluoro-2-(1H-1,2,4-triazol-1-yl)acetophenone, 85 mg (yield 15%) of the title compound, melting at 100°-101° C., were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134152 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-bc2aaa7144b24cb3848d25e8837f2293 |
| Source note | uspto-grants-1992_07 |