HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → HCID 178438938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | HCID 178438938 | HCID 178438938 | — |
Reaction Steps
Methacrylic acid (6.88 g; 80 mmole) was dissolved in dry tetrahydrofuran (40 ml), and triethylamine (8.0 g; 80 mmole) and thiophenol (8.81 g; 80 mmole) were successively added thereto at room temperature, followed by stirring for 24 hours. Removal of the solvent under reduced pressure gave 2-methyl-3-phenylthiopropionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134231 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-b4d245a210164760a316806f5c8411b9 |
| Source note | uspto-grants-1992_07 |