HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86638830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 59185401 | HCID 59185401 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86638830 | HCID 86638830 | — |
Reaction Steps
To a solution of (2S)-2-[(tert-butoxycarbonyl)-amino]-propyl pivaloate (1.0 eq.) in EtOAc (0.6 M) was added 4N HCl in dioxane (10 eq.). The reaction mixture was stirred for 2.5 h and then the solvent was evaporated in vacuo to give a solid that was washed with Et2O and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071568B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-16a40a4ffab941b18951a14abaa35f13 |
| Source note | uspto-grants-2011_12 |