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HRID65521

反应详情

EQUATION

反应方程式

HRID 65521 的结构方程式

REACTANTS

反应物

2
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：CC(C)(C)NCC(=O)c1ccc(O)c(O)c1.Cl
HCID3015704

1-(3,4-Dihydroxyphenyl)-2-((1,1-dimethylethyl)amino)ethan-1-one hydrochloride

C12H18ClNO3

PRODUCTS

生成物

1
结构：Cc1ccc(Oc2ccc(C(=O)CNC(C)(C)C)cc2Oc2ccc(C)cc2)cc1.Cl
HCID70467733

未命名化合物

收率 64%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

The process of Example 1 was repeated substituting acetone for the acetonitrile as solvent. Starting with 26 g of 3,4-dihydroxyphenyl N-(tert-butyl)aminomethyl ketone hydrochloride there was obtained 33 g of 3,4-bis-(p-toluyloxy)phenyl N-(tert-butyl)aminomethyl ketone hydrochloride (64% yield) containing only a trace of tributylamine hydrochloride.