HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 2-[4-(2-fluorophenoxy)phenyl]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-[4-(2-Fluorophenoxy)phenyl]propionic acid | HCID 20559786 | — |
| Product | Ethyl 2-[4-(2-fluorophenoxy)phenyl]propionate | HCID 22757306 | — |
Reaction Steps
2-[4-(2-Fluorophenoxy)phenyl]propionic acid (2.32 g.) in ethanol (16 ml.) containing concentrated sulfuric acid (0.5 ml.) were refluxed for 5 hours and the alcohol removed. After dilution with water the product was isolated in ether and distilled to give ethyl 2-[4-(2-fluorophenoxy)phenyl]propionate, b.p. 176°-177° C./2.5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04128573 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-33bd4a495d2f4ef996180e7466d31fac |
| Source note | uspto-grants-1978_12 |