HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxypropyl)triphenyl-phosphonium iodide → 6-Bromo-3-methoxy-2-(4-methoxybut-1-enyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxypropyl)triphenyl-phosphonium iodide | HCID 20084049 | — |
| Reactant | 6-Bromo-3-methoxypyridine-2-carbaldehyde | HCID 70700415 | — |
| Product | 6-Bromo-3-methoxy-2-(4-methoxybut-1-enyl)pyridine | HCID 86639840 | — |
Reaction Steps
1.5 mmol of 6-bromo-3-methoxypyridine-2-carbaldehyde and (3-methoxypropyl)triphenyl-phosphonium iodide [133622-76-1] are reacted in analogy to building block 24a. The title compound is identified by means of the Rf.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071651B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-40b01454f09e402b907fe7a6a7d2e3f2 |
| Source note | uspto-grants-2011_12 |