HuagongsheHuagongshe Chemistry Print Report · For research reference only
38263-46-6 → HCID 55300761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 38263-46-6 | HCID 9833980 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 55300761 | HCID 55300761 | — |
Reaction Steps
A solution of 1 mmol of (1S,2R,4S)-7-oxabicyclo[2.2.1]-hept-5-ene-2-carboxylic acid [185840-15-7] in 30 ml of ethanol is hydrogenated in the presence of 0.150 g of Pd/C 10% at room temperature until conversion is complete. The reaction mixture is clarified by filtration, and the filtrate is evaporated. The title compound is obtained from the residue by flash chromatography (SiO2 60 F).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071651B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-04eaa553a8774abab23d4618f0b453fb |
| Source note | uspto-grants-2011_12 |