HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69231152, compound → HCID 69230028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69231152 | HCID 69231152 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69230028 | HCID 69230028 | — |
Reaction Steps
Compound 22-7 (150 mg) and 10% palladium/carbon (catalytic amount), together with methanol (10 ml), were poured into reactor and the reactor was filled with hydrogen gas, followed by stirring at room temperature for 24 hours. After the completion of the reaction, the resulting mixture was filtered through celite and concentrated under reduced pressure. The following procedure was carried out using the obtained residue which was not purified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071650B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-c148d03891eb44a0a1ae87efaeb68fde |
| Source note | uspto-grants-2011_12 |