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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 656301Generated: October 29, 2026

HCID 69231152, compound → HCID 69230028, compound

https://huagongshe.com/reaction/656301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69231152HCID 69231152—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 69230028HCID 69230028—

Reaction Steps

Compound 22-7 (150 mg) and 10% palladium/carbon (catalytic amount), together with methanol (10 ml), were poured into reactor and the reactor was filled with hydrogen gas, followed by stirring at room temperature for 24 hours. After the completion of the reaction, the resulting mixture was filtered through celite and concentrated under reduced pressure. The following procedure was carried out using the obtained residue which was not purified.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08071650B2
Source datasetuspto-grants-2011_12
ORD IDord-c148d03891eb44a0a1ae87efaeb68fde
Source noteuspto-grants-2011_12