Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 656438Generated: November 3, 2026

Ammonia → HCID 22228384, compound

https://huagongshe.com/reaction/656438

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 86015016HCID 86015016—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 22228384HCID 22228384—

Reaction Steps

5-Piperidin-1-ylindan-1-one O-methyloxime (2.95 g, 12 mmol), 10% palladium on carbon (1.45 g), and 20% ammonia in methanol (80 ml), were placed in a Parr apparatus, which was charged with hydrogen to 60 psi. The mixture was shaken for 1 hour at ambient temperature and filtered. The filtrate was removed under vacuum to provide the title compound which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08071762B2
Source datasetuspto-grants-2011_12
ORD IDord-1b803bc2fcf743539c676f34dd52b808
Source noteuspto-grants-2011_12