HCID 66915443, compound → HCID 178487333, compound

Participants

Reaction Steps

A solution of 1 mmol of 4-(1-benzyl-1H-imidazol-4-yl)-4-(3-benzyloxypropyl)-7-methoxychroman-2-one in 15 ml of methanol and 2 ml of conc HCl is hydrogenated in the presence of 100 mg of 10% Pd/C at 15° C. for 10 hours. The reaction mixture is subjected to clarifying filtration and the filtrate is evaporated. The crude title compound is identified on the basis of the Rf value and reacted further without further purification.

Provenance & Evidence