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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 656493Generated: November 2, 2026

Dimethylformamide dimethyl acetal → HCID 66915648, compound

https://huagongshe.com/reaction/656493

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
ReactantHCID 66915531HCID 66915531—
SolventDichloromethaneHCID 6344—
ProductHCID 66915648HCID 66915648—

Reaction Steps

A solution of 31 mmol of 1-(6-methoxyspiro[1-benzofuran-3,3′-piperidin]-2′-yl)methanamine and 31 mmol of N,N-dimethyl formamide dimethylacetal in 50 ml of dichloromethane is heated to reflux for 6 hours. The reaction mixture is cooled to room temperature and evaporated. The crude title compound is identified on the basis of the Rf value and reacted further without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08071774B2
Source datasetuspto-grants-2011_12
ORD IDord-4128eef8d5034ed6b61d76acd6f33747
Source noteuspto-grants-2011_12