HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 66915648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 66915531 | HCID 66915531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66915648 | HCID 66915648 | — |
Reaction Steps
A solution of 31 mmol of 1-(6-methoxyspiro[1-benzofuran-3,3′-piperidin]-2′-yl)methanamine and 31 mmol of N,N-dimethyl formamide dimethylacetal in 50 ml of dichloromethane is heated to reflux for 6 hours. The reaction mixture is cooled to room temperature and evaporated. The crude title compound is identified on the basis of the Rf value and reacted further without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071774B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-4128eef8d5034ed6b61d76acd6f33747 |
| Source note | uspto-grants-2011_12 |