HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24800231, compound → HCID 57557577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24800231 | HCID 24800231 | — |
| Reactant | 6-bromo-4-(trifluoromethyl)picolinaldehyde | HCID 59635571 | — |
| Product | HCID 57557577 | HCID 57557577 | — |
Reaction Steps
Was synthesized in the same manner as 2-cyclopropyl-6-(((4-(4-fluorophenyl)-1-methylpiperidin-4-yl)methoxy)methyl)-4-(trifluoromethyl)pyridine starting from 6-bromo-4-(trifluoromethyl)picolinaldehyde. 1H-NMR (CDCl3, 400 MHz) δ 9.99 (s, 1H), 7.87 (s, 1H), 7.56 (s, 1H) 2.18 (m, 1H), 1.20 (m, 4H). LC: Tr=1.84 min, HPLC Method 1. Mass spec.: 216.37 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071778B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-ec4b05f6865e4f108f17b39d9d47b920 |
| Source note | uspto-grants-2011_12 |