HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinemethanol → Phthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinemethanol | HCID 7510 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Product | Phthalimide | HCID 6809 | 81.3% |
Reaction Steps
Phthalimide-protected intermediate 2G was prepared from pyridin-3-ylmethanol and N-hydroxyphthalimide by a procedure analogous to Example 2A, Step 1 (3.22 g, 81.3% yield). ESI-MS: m/z 255.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071766B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-6345d91ae214497ca79c72e1d29ff0f8 |
| Source note | uspto-grants-2011_12 |