Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2,2,2-Trifluoro-1-methoxyethanol | HCID 9892 | — |
| Reactant | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | — |
| Product | HCID 86050515 | HCID 86050515 | — |
Reaction Steps
This reaction was carried out in essentially the same manner as described in Example 1 using charges of sulfuric acid (175 g), (CF3)2CHOH (70.6 g, 0.42 mole, Synquest Labs) and trifluoroacetaldehyde methyl hemiacetal (Alfa Aesar, 50 g, 90% purity, 0.346 mole). In this case the receiver was cooled in an ice water bath to about 0° C. to avoid solidification of the alcohol. The receiver had gained 8.6 g in weight and this solution was used without purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08071816B2 |
|---|
| Source dataset | uspto-grants-2011_12 |
|---|
| ORD ID | ord-cd1913e3086d4c10a73cc1e2b0e2702c |
|---|
| Source note | uspto-grants-2011_12 |
|---|
