Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 3-Hydroxy-4-methoxybenzeneacetic acid | HCID 160562 | — |
| 생성물 | Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate | HCID 5324706 | — |
반응 단계
To 3-hydroxy-4-methoxyphenylacetic acid (5.0 g, 23.8 mmol) in EtOH (100 mL) was added sulfuric acid (1 mL), and the reaction was stirred overnight at room temperature. Once no starting material was seen by analytical tlc, the mixture was concentrated to give the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08071807B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-aae79e58cbb64033a00675bea423e808 |
| 출처 메모 | uspto-grants-2011_12 |