HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68809572, compound → 7-Methoxy-1,2-dihydroquinolin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68809572 | HCID 68809572 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 7-Methoxy-1,2-dihydroquinolin-2-one | HCID 29942756 | 60.6% |
Reaction Steps
(2E)-3-(Ethyloxy)-N-[3-(methyloxy)phenyl]-2-propenamide (25 g; 0.113 mol) was dissolved in conc. H2SO4 and stirred for 1 h. The reaction mixture was poured onto ice and filtered. The crude product was washed with water and dried to yield the title compound (12 g; 60%) as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071592B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-fe817eb91bf8491cbb6cd5145a3fa0a4 |
| Source note | uspto-grants-2011_12 |