HRID657025

反应详情

EQUATION

反应方程式

HRID 657025 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate (1 g, 2.21 mmol) was added 20% Pd(OH)2/C, degassed and placed under 1 atm of H2 for 2 h. The reaction mixture was filtered through Celite and concentrated to obtain the title compound as a yellow oil (622 mg, 89%).

WORKUP

后处理

  1. customdegassed
  2. filtrationThe reaction mixture was filtered through Celite
  3. concentrationconcentrated