HRID657093

反应详情

EQUATION

反应方程式

HRID 657093 的结构方程式

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

Hydrogen chloride gas was bubbled into a solution of 2-({4-amino-6-chloro-2-[(E)-2-phenylethenyl]-5-pyrimidinyl}oxy)acetamide (0.6 g, 1.97 mmol) in ethanol (20 mL). The resulting mixture was heated at 100° C. for 3 h. The mixture was evaporated under reduced pressure to give the desired product as a solid (0.55 g, 84%) which was used without purification.

WORKUP

后处理

  1. customThe mixture was evaporated under reduced pressure