HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(2,3-dichlorophenyl)propionate → 3-(2,3-Dichlorophenyl)propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(2,3-dichlorophenyl)propionate | HCID 12595092 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 3-(2,3-Dichlorophenyl)propanoic acid | HCID 12595101 | — |
Reaction Steps
Methyl 3-(2,3-dichlorophenyl)propionate was refluxed in 10% aqueous sodium hydroxide (1 l.) for two hours and the reaction mixture was cooled, acidified and filtered. The filter cake was dissolved in hot aqueous sodium bicarbonate, and filtered. The filtrate was acidified and filtered to yield 3-(2,3-dichlorophenyl)propionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04128666 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-000a1bced82f4a62a15526285accafb3 |
| Source note | uspto-grants-1978_12 |