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HRID657441

反应详情

EQUATION

反应方程式

HRID 657441 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1cc(=O)[nH]c(=O)[nH]1
HCID967

Orotic acid

C5H4N2O4

结构：CN(CC(=O)O)C(=N)N.O
HCID80116

Creatine monohydrate

C4H11N3O3

PRODUCTS

生成物

1
结构：CN(CC(=O)O)C(=N)N.CN(CC(=O)O)C(=N)N.CN(CC(=O)O)C(=N)N.O=C(O)c1cc(=O)[nH]c(=O)[nH]1
HCID11444210

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Under room temperature 447 grams of creatine monohydrate is slowly added to 3.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with alcohol. After drying 555 grams of Tricreatine orotate is obtained.

WORKUP

后处理

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 555 grams of Tricreatine orotate
  5. customis obtained