HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → HCID 17973399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 5364373 | HCID 5364373 | — |
| Product | HCID 17973399 | HCID 17973399 | 69% |
Reaction Steps
3-(3-Cyclohexenyl)-2E-propenoic acid 1 eq, ethyl chloroformate 1.5 eq, triethylamine 1.5 eq, cyclopropylamine 1.6 eq, quench with 10% sodium chloride solution, yield=69%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08075937B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-4aed42a36dbd4166904bb68305f98850 |
| Source note | uspto-grants-2011_12 |