HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl iodide → HCID 86761473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl iodide | HCID 85247 | — |
| Reactant | HCID 86761458 | HCID 86761458 | — |
| Reactant | HCID 86761475 | HCID 86761475 | — |
| Product | HCID 86761473 | HCID 86761473 | 73% |
Reaction Steps
This compound was prepared as described for 3f, using 22 (200 mg, 0.53 mmol) as a starting material and iodotrimethysilane (0.6 mL, 4.2 mmol). Compound 3h (130 mg, 0.38 mmol) was obtained as a colorless solid, in 73% yield, which was characterized as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076310B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-8fff611083844e4a9128a18d7b80cdd3 |
| Source note | uspto-grants-2011_12 |