HCID 68531843, compound → HCID 68529618, compound

Participants

Reaction Steps

1.5 g (8.65 mmoles) of the product of Step 1 are dissolved in 30 mL of methanol (MeOH). 30 mL of a (7N) ammoniacal methanol solution and 0.5 g of Raney nickel. The reaction mixture is then hydrogenated overnight under a pressure of 1 bar, at ambient temperature. The catalyst is then filtered off and the filtrate is evaporated to dryness. The expected product is obtained in the form an oil.

Provenance & Evidence